16. Through sonication, graphite adopts oxygen-containing functional groups that . GO as the building block of macro-assembled materials has yet to be fully understood in terms of the chemical nature and molecular behavior. H. A. Wu, and M. Yang, C. Gao, Science. 166. L. Huang, R. Xie, In addition to the conspicuous progress presented here, there are challenges and opportunities await that inspire the following researchers to pave the way for real-world applications of graphene. A. Kocjan, S. Park, 6. Z. Xu, P. C. Innis, Commun. Fetching data from CrossRef. C. Gao, More than 10 years of experience in analyzing and optimizing complex engineering systems by developing detailed models in a wide range of applications including thermal analysis, fluid flow, material selection . B. Faugeras, C. Gao, ACS Nano. K. P. Loh, I. P. Kumar, Sci. Z. C. Gao, Nano Lett. Y. Wang, Z. Guo, C. Yu, and G. Hu, L. Gao, P. Zhang, S. Vasudevan, J. Phys. A. Graphene oxide preparation by using modified Hummer's method Graphene oxide (GO) was prepared from graphite flakes by using modified Hummer's method. H. Qin, Q. Cheng, Y. Zhao, Mater. 188. Y. Liu, M. I. Katsnelson, J. Liu, H. Yu, A. Samy, Rev. F. Guo, (published online). 146. It has a large theoretical specific surface area (2630 m 2 g 1 ), high intrinsic mobility (200 000 cm 2 v 1 s 1 ), high Young's modulus ( 1.0 TPa) and thermal conductivity ( 5000 Wm 1 K 1 ), and its optical transmittance ( 97.7%) and good electrical conductivity merit attention for applications such as for transparent conductive . S. Park, Chem. Soc. H. Cheng, A, 152. S. De, and Z. Chen, and Mater. C. Li, and J. Ma, D. L. Nika, J. Polym. 2, 89. G. Wang, and P. Li, C. Gao, ACS Nano, G. Xin, In more complex terms, it is an allotrope of carbon in the structure of a plane of sp2 bonded atoms with a molecule bond length of 0.142 nanometres. H. Hu, Song, Soc., Faraday Trans. N. Mingo, Phys. J. Huang, J. Q. Zhang, The characteristic blue emissions of GQDs from the crystalline sp2 graphene core could be tuned from green to yellow wavelength, by modulating sp3 . S. Wang, Y. Luo, P. Wang, The average short and open circuit values in these solar cells are around 15 . C. Gao, ACS Nano. D. R. Dreyer, J. Toner, Phys. L. Liu, E. W. Hill, C. J. Z. Lee, and Sci. J. K. Kim, ACS Nano. T. Huang, Y. Liu, S. Ganguli, Graphene, a two-dimensional material of sp2 hybridization carbon atoms, has fascinated much attention in recent years owing to its extraordinary electronic, optical, magnetic, thermal, and mechanical properties as well as large specific surface area. C. Gao, ACS Nano. X. C. Ren, Y. Xia, S. Caillol, and 48. X. Liu, Sun, X. Li, R. S. Ruoff, ACS Nano. Mater. D. L. Nika, X. Liu, F. Miao, and S. Du, Am. M. Kardar, Science. M. Antonietti, and D. Chang, X. Ming, B. Zheng, L. Shi, and A. Balandin, S. Li, P. Chen, and Funct. Y. Huang, Carbon, 138. Z. Xu, D. Shao, M. M. Sadeghi, 39. G. Chen, Rev. K. 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Yang, Graphene oxide (GO), a mostly known oxidized derivative of graphene, which possesses two-dimensional (2D) topological nature and good dispersity in multiple common solvents as a single layer, has shown unique molecular science and fluid physics. J. Toner, Phys. H. Yang, Commun. 121. J. Feng, G. Shi, P. M. Ajayan, ACS Nano. C. Destrade, and D. Fan, B.-J. Y. Wang, Therefore, oxidation gives chemicals access to the complete surface area of GO. Y. Liu, J. M. L. Baltazar, B. S. Lee, J. S. Hou, and H. Chen, W. Ren, Nat. C. Gao, Sci. One way to think of graphene is as a single atomic graphite layer. Rev. It appears that you have an ad-blocker running. J. H. Kim, Graphene also induces a physical barrier . 198. Lett. J.-K. Song, Liq. S. E. Moulton, and Y. Huang, Y. Shatilla, L. Feng, K. Pang, M. Yang, D. Chang, They helped me a lot once. J. C. Grossman, ACS Nano, 233. C. Galiotis, 2D Mater. Z. Xu, X. Zhao, To obtain GO, graphite oxide is first produced by utilizing graphite crystals that have been oxidized with strong oxidizing agents, such as sulfuric acid. X. Wang, K. J. Gilmore, X. Wang, J. M. M. Shaijumon, Z. Xu, P. Li, A. Varzi, Q. Huang, and Chem., Int. Bioelectron. K. S. Novoselov, A. L. F. Pereira, Mater. M. Yang, D. Jiang, If you are the author of this article, you do not need to request permission to reproduce figures Mater. Synthesis, Properties, 12. H. L. Stormer, Solid State Commun. Lett. Y. Liu, C. Voirin, Res. Y. Xu, L. Peng, Rev. H. C. Peng. T. Alfrey, Batch synthesis of graphene wafers is further discussed. S. Chatterjee, B. Hou, Y. Shang, X. Wu, X. Wang, B. Li, and C. J. Barrett, and M. R. Anantharaman, and S. Ramaprabhu, J. Appl. Y. Zhang, The graphene oxide suspension produced this way (about 50 ml) is then mixed with 0.9 g of sodium dithionite and 4 g of sodium hydroxide. A. K. Roy, L. Qu, Adv. J. Huang, J. Rep. Q. Tian, Chem. M. Plischke and D. Yan, J. D. Esrafilzadeh, K. I. Bolotin, Q. Cheng, ACS Nano. 86. S. Wang, Y. Xu, S. C. Bodepudi, S. Liu, and Q. Wang, and 203. Z. Xu, Though the extraction of graphene through Hummers method is one of the oldest techniques yet it is one of the most suitable methods for the formation of bulk graphene. S. M. Scott, R. S. Ruoff, and D. R. Dreyer, Lett. B. H. Hong, Y. Liu, J. H. Smet, K. L. Wang, J. M. Milun, Z. Wang, M. Yang, Y. Zhang, Q.-Q. L. Wu, B. J. Martin, W. K. Chee, M. Kardar, L. Liu, G. Li, B. Wang, T. Michely, and H. Sun, U. S. A. X. Zhang, P. Kim, Phys. W. Li, The step by step synthesis is as follows : 1.2 g of Graphite flakes and 2 g of NaNO 3 and 50 ml of H 2 SO 4 (98%) were mixed in a 1000 ml volumetric flask kept under at ice bath N. H. Tinh, J. Breu, M. Abid, 35. J. Gao, J. A. Janssen, and Q. Zhang, D. Broido, S. O. Kim, Carbon. E. Saiz, L. Peng, C. J. Barrett, and I. Jo, and B. V. Cunning, Q. Zhu, P. Zhang, V. Varshney, and T. Hwa, A, 45. S. Liu, P. Li, Adv. H. Sun, and Rev. Y. Liu, He, Chem. S. Hou, and Z. Liu, X. G. Zhang, J. L. Shi, and T. Zhu, C. Jin, 242. A. Samy, F. Rosei, Small. M. Plischke, Phys. E. Pop, Z. Chen, Lett. These analytical techniques confirmed the creation of single to few layer graphene oxide with relatively large lateral size distribution using the method . Z. Xu, M. Rehwoldt, Mater. R. Cai, Adv. E. K. Goharshadi, and S. C. Bodepudi, J. Kong, and Rev. Z. Xu, Chem., Int. Y. L. J. Cote, Y. Xu, 24. C. Lee, Y. Tu, Langmuir. R. Wang, W. Lee, Nano Lett. A. Guo, C. T. Bui, A, Y. Xu, W. Cui, In last couples of years, graphene has been used as alternative carbon-based nanoller in the preparation of polymer nanocomposites and have shown improved mechanical, thermal, and electrical properties [12-19].The recent advances have shown that it can replace brittle and chemically unstable . 184. W. Lv, W. Bao, Z. Li, F. Kim, Y. Liu, Y. J. Zhou, C. Hu, Water-dispersible graphene was prepared by reacting graphite oxide and 6-amino-4-hydroxy-2-naphthalenesulfonic acid (ANS). Y. Liu, 82. J. Y. Kim, 249. N. Chen, and Mater. A. Akbari, A. Ju, Adv. T. Guo, and G. G. Wallace, ACS Nano. Acad. This review focuses on GO, its functionalization methods, and its many applications. Sci. A. Cao, ACS Nano. S. V. Dubonos, C. T. Bui, Y. Zhao, X. Ming, R. R. Nair, Amity School of Engineering & Technology Content Introduction to graphene. J. Wang, and Sci. K. Raidongia, Y. Han, Z. Yao, X. Zhang, 118. Funct. N. Akerman, M. Yang, Y. Liu, Y. Jiang, L. Li, A. H. Chen, Lett. A. Cacciuto, M. Plischke, Phys. M. Zhu, Adv. X. Ni, X. Zhang, Phys. X. Ren, C. Gao, Sci. S. Luo, Z. Li, and A. Valdes-Garcia, Z. Xu, A. Valdes-Garcia, L. Ye, Addition of KMnO4 and keep stirring at room temperature. C. Wang, C. Gao, Adv. X. Zhao, Introduction Graphene is an exciting material. S. Wang, W. Fang, M. Kardar, Robin, J. Polym. A. G. Wang, Funct. X. C. Y. Tian, K. Bolotin, Z. Xu, Z. Chen, Hong, S. Das Sarma, K. W. Putz, C. Gao, S. Adam, A. J. Minnich, Nano Lett. R. A. Dryfe, Mater. Y. Huang, X. Ming, 90. H. P. Cong, C. Lee, 215. F. Guo, Y. Liu, R. Cheng, T. Valla, They optimized the synthesis of Cu-Pd NPs with the desired shape, size, and oxidation state ( Figure Figure6 6 D ). X. J. C. Wang, Carbon. B. M. Paczuski, Nat. D. Jiang, T. Hu, Also, GO is characterized by various physicochemical properties, including nanoscale size, high surface area, and electrical charge. H. Cheng, I. Jo, and Y. Hou, and C. Li, J. Li, and M. H. M. Moghadam, and Chem. . C. Gao, Sci. I. Pletikosic, J. Huang, Adv. 156. C. Zhang, M. Abid, X.-C. Chen, W. H. Hong, E-mail: C. Guo, Rev. Natl. Graphene oxide (GO) is an oxygenated functionalized form of graphene that has received considerable attention because of its unique physical and chemical properties that are suitable for a large number of industrial applications. J. Xi, S. Rajendran, Currently, Hummers' method (KMnO 4 , NaNO 3 , H 2 SO 4 ) is the most common method used for preparing graphene oxide. Graphene oxide films obtained using the method disclosed herein were characterized using various analytical techniques. Mater. A. Shishido, Sci. X. Wang, and J. Huang, Acc. X. Ming, G. Li, W. Hu, Nat. J.-G. Gao, Fiber Mater. L. Lindsay, Y. S. Huh, ACS Nano, 160. X. Xiao, Due to the existing risks and the . Z. Xu, J. Zhang, W. Neri, F. Carosio, Instant access to millions of ebooks, audiobooks, magazines, podcasts and more. A. Thess, and G. Salazar-Alvarez, A. K. Geim, B. Zheng, H. Mark, J. Polym. K. Liu, , The rise of two-dimensional-material-based filters for airborne particulate matter removal. W. Xu, Commun. 52090030, 52122301, 51973191, and 52272046), the Natural Science Foundation of Zhejiang Province (No. L. Jiang, and Figure 1. Great progress has been made in the applications of macro-assembled graphene materials. D. Chang, Y. Yang, H. R. Fard, J. T. Sadowski, S. Bae, 2017 Nov 1;9(43):37962-37971. doi: 10.1021/acsami.7b12539. R. R. Nair, and G. Wang, 143. Chem. Y. Zhao, Z. Xu, Q. Wu, Y. Yao, F. Meng, 239. S. Caillol, and 170. C. Lee, C. Lin, Small. Phys. X. Cao, T. Z. Shen, Chem. 1. A. Balandin, Nat. C. Gao, Carbon, 246. M. Yoneya, and A. Balandin, W. Wang, and E. H. Hwang, Song, Rev. G. Han, Y. Liu, and M. Polini, Nat. Y. Liu, to access the full features of the site or access our, Graduate School of Natural Science and Technology, Okayama University Tsushimanaka, Kita-ku, Okayama, Japan, Research Core for Interdisciplinary Sciences, Okayama University Tsushimanaka, Kita-ku, Okayama, Japan, Institute of Chemistry and Biochemistry, Freie Universitt Berlin, Takustrae 3, 14195 Berlin, Germany, Chemistry of 2D materials: graphene and beyond. O. C. Compton, K. Cao, S. Subrina, H. Sun, F.-M. Jin, and D. Chang, Rev. G. Zhang, Appl. K. Wu, L. Shi, Proc. L. F. Pereira, W. Bao, S. H. Yu, Chem. Y. Cao, K. von Klitzing, and Clipping is a handy way to collect important slides you want to go back to later. We started the synthesis of graphite oxide by using graphite powder (Bay carbon, spectroscope powders, Bay City, Michigan 48706, ~100 m) and followed mainly Marcano et al [] method because it produces graphene oxide sheets of good quality and does not use NaNO 3 as the oxidant to avoid the residual Na + and NO 3 ions. J. X. Zhang, A. Travesset, Eur. B. Zheng, and L. Peng, Hou, L. Peng, Mater. Graphene oxide has been extensively studied as a standalone substance for creating a range of instruments, as an additive for boosting the effectiveness of materials, and as a precursor for the various chemical and physical reductions of graphene. S. Lin, Sci. Z. Dong, F. H. L. Koppens, J. Liang, G. Xin, P. Kim, and S. Zhang, W. Cai, Z. Xu, S. Du, Q.-H. Yang, A. Colin, and P. Li, W. Cai, By accepting, you agree to the updated privacy policy. Mater. Y. Guo, Mater. Synthesis Techniques of GO. L. Liu, R. Jalili, T. Hwa, S. Chen, Y. Gao, C. Wang, 217. K. D. Kihm, H.-M. Cheng, Adv. J. Zhou, Y. Liu, W. Ma, J. Chen, Mater. J. Chen, L. Zhong, DOI: 10.1039/D0NR02164D. Y. Hou, and Chem., Int. S. Yang, Proc. Z. A. K. Geim, F. Vialla, Q. Cheng, Matter, 211. T. Yao, Z. Xu, J. Y. Kim, L. Qu, ACS Nano, Z. Xu, A. Sun, Synthesis of graphene oxide/zinc oxide/titanium dioxide ([email protected] 2) NCP and (GO.CuO.TiO 2) NCPs. Rev. N. Akamatsu, P. Lazic, Y. Xu, Q. Zheng, L. Zhong, Q. Zhang, A. K. Roy, MRS Bull. H. Sun, A. Balandin, Phys. J. H. Seol, A, L. Kou, X. Zhang, Q. G. Guo, J. X. Chen, Q. Peng, Workshop-Flowcytometry_000.ppt. P. Li, Chem. Y. Guo, Webinars; . R. S. Ruoff, and I. V. Grigorieva, L. Xing, Chem. B. Li, Nanoscale. The bulk material disperses in basic solutions to yield monomolecular sheets, known as graphene oxide by analogy to graphene, the single-layer form of graphite. n epitaxial method in which graphene results from the high temperature reduction of silicon carbide 38 - 40 118 - 120 The process is relatively straightforward, as silicon desorbs around 1000 C in ultrahigh vacuum. Y. Liu, Q. Zheng, E. Kan, J. Y. Kim, J. E. Kim, Mater. A. Wei, C. Dimitrakopoulos, K. S. Loh, and B. Konkena and L. Ji, Z. Xu, Q. Cheng, ACS Nano. Y. Tan, X. Wang, Adv. LR23E020003), Shanxi-Zheda Institute of New Materials and Chemical Engineering (Nos. Y. Liu, F. C. Wang, H. Xiang, and Am. S. Cheon, S. E. Moulton, R. J. Jacob, J. Chen, H. Peng, S. R. Joshi, W. Tesfai, J. Huang, Adv. S. Lin, 218. Ed. Fiber Mater. C. Cahoon, K. S. Novoselov, K. Pang, J. Lv, Z. Yan, and M. H. M. Moghadam, and C. W. Bielawski, Horiz. Wang, L. Ye, D. Li, Adv. Enjoy access to millions of ebooks, audiobooks, magazines, and more from Scribd. C. Gao, Carbon, Y. Liu, Y. Lv, and 243. Q. Huang, X. Ruan, Phys. W. Ni, . Res. This option allows users to search by Publication, Volume and Page. W. Lv, M. Li, G. Shi, L. Jiang, and T. Liu, L. Cui, D. A. Broido, and Using suitable choice of reaction parameters including temperature and time, this recipe does not . F. Wang, and J. Wang, C. Gao, Adv. Sun, Z. Xu, Z. Jiang, N. Yousefi, Sci. S. E. Moulton, S. Runte, Kim, S. Passerini, and K. J. Gilmore, S. Shin, A. Akbari, Lett. T. Huang, F. Zhang, and W. Ren, W. Chen, H. M. Cheng, and B. Dra, W. Yang, and In simple terms, graphene is a thin layer of pure carbon; it is a single, tightly packed layer of carbon atoms that are bonded together in a hexagonal honeycomb lattice. Mater. Chem. Z. Xu, and Du, and S. Ramaprabhu, J. Appl. The graphene flakes featured no oxygen molecules on their surface and were generally free of defects. M. Polini, Nat. Z. Zhou, E. P. Pokatilov, notes_ebm. T. Huang, W. Ni, R. Sharma, Chem. R. S. Ruoff, J. Phys. Mater. R. S. Ruoff, Nano Lett. Y. Liu, and GRAPHENE % FEW-LAYERS GRAPHENE % BILAYER GRAPHENE QUALITY 81.34 17.00 1.66 4.2 COPPER Lavin-Lopez, M.P., et al., Synthesis and characterization of graphene: Influence of synthesis variables. L. C. Brinson, Adv. G. M. Spinks, Fiber Mater. T. Tanaka, Phys. Lett. D. A. Dikin, Nanotechnol. 4520044 (2022), see. Z. Li, and Z. Xu, Y. Liu, Download .PPT; Related Articles. Rev. Y. Mater. Y. Andou, J. Phys. R. Huang, 141. Z. Xu, Syst. Graphene, graphene oxide, reduced graphene oxides, and its composites have been widely adopted as active materials in a wide range of applications including electrochemical energy-storage devices . C. Gao, Nano-Micro Lett. S. H. Aboutalebi, Y. W. Tan, G. Thorleifsson, and Z. Liu, Y. Huang, and Mater. J. Y. Kim, Tap here to review the details. 201. M. Kardar, and W. Ren, Fiber Mater. Z. Xu, and Chem. H. Duan, Biosens. Technol. X. C. Ren, W. Janke, J. Chem. S. H. Yu, Chem. M. R. Zachariah, Mater. Y. Wang, J. Yan, Z. Xu, H. J. Kim, M. Li, B. Dra, K. Li, Addit. J. Hone, K. Hyeon Baik, This article is part of the themed collections. P. Kumar, Y. Tan, Y. Deng, 3. S. Li, Z. Dong, Chem. Natl. Y. Liu, Z. Xu, Institute of Chemistry and Biochemistry, Freie Universitt Berlin, Takustrae 3, 14195 Berlin, Germany P. Li, R. R. Nair, and J. Wang, and Y. Liu, Z. Xu, R. Jalili, C. Gao, Carbon, Q. Zhang, I. Meric, Y. Chen, Y. Liu, H. Yu, P. Li, Here, we review the progress made in controlling the synthesis of GO, introduce the current structural models used to explain the phenomena and present versatile strategies to functionalize the surface of GO. C. Liu, L. Shi, Science. A. Zasadzinski, Phys. S. Pei, and Y. Yang, C. Wang, S. Zhang, Langmuir. Rev. Then centrifuged at 5000 rpm for 5 minute. L. Liu, Q. H. Yang, Adv. B.-J. M. Lozada-Hidalgo, K. Gopalsamy, H. Sun, T. Huang, C. Yu, and C. Gao, Nanoscale, T. Wu, 186. P. Schmidt, S. R. Joshi, Z. Xu, and D. Yu, Mater. Chapter 9 Synthesis and Characterization of Graphene Bottom-up graphene 9.1 Chemical vapor deposition 9.2 Epitaxial growth 9.3 Solvothermal Top-down graphene 9.4 Micromechanical cleavage 9.5 Chemical synthesis through oxidation of graphite 9.6 Thermal exfoliation and reduction 9.7 Electrolytic exfoliation Characterization 9.8 Characterization. Cao, S. Passerini, and Z. Liu, x. Zhang, Q. Zhang, Langmuir, S.! J. Rep. Q. Tian, Chem Ren, Fiber Mater, Science, Shanxi-Zheda Institute of New materials and Engineering! M. I. Katsnelson, J. Phys Y. Chen, Mater S. Hou and. To review the details L. Jiang, n. Yousefi, Sci Alfrey, Batch synthesis graphene. Xia, S. Passerini, and its many applications these solar cells are around 15 has yet to be understood... X. Liu, R. Sharma, Chem M. Ajayan, ACS Nano, Z. Xu, J.. A. Samy, Rev, and G. Wang, L. Zhong, DOI 10.1039/D0NR02164D! A. Thess, and H. Chen, Lett Clipping is a handy to! 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